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Diesel engines are very efficient prime movers in their power range. Fuel is directly injected into the combustion chamber. Performance and emission characteristics of diesel engines are highly influenced by the fuel spray parameters and atomization of the injected fuel. As the emission regulations become stringent, it is very important to optimize the combustion in internal combustion engines for different fuels including alternative fuels. Spray visualization using optical techniques play a very important role to analyze macroscopic spray parameters and fuel atomization behavior. In the present experimental study, an important alternative CI engine fuel, Karanja oil and its blends with diesel have been investigated for their spray parameters and fuel atomization relative to mineral diesel. These parameters are different for the two fuels because of difference in the viscosity and density of the fuels.