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Direct osmotic concentration (DOC) is an integrated membrane treatment process designed for the reclamation of spacecraft wastewater. The system includes forward osmosis (FO), membrane evaporation, reverse osmosis (RO) and an aqueous phase catalytic oxidation (APCO) post-treatment unit. This document describes progress in the third year of a four year project to advance hardware maturity of this technology to a level appropriate for human rated testing. The current status of construction and testing of the final deliverable is covered and preliminary calculations of equivalent system mass are funished.

The Vapor Phase Catalytic Ammonia Removal (VPCAR) Technology has undergone long duration testing at MSFC. The results of this testing revealed several areas in which the VPCAR Technology could be improved and those improvements are summarized here. These improvements include the replacement of several parts with units that are more durable, redesign of several pieces which proved to have mechanical weaknesses, and incorporation of some new designs in order to prevent other potential problems.

The Lightweight Contingency Water Recovery System (LWC-WRS) harvests water from various sources in or around the Orion spacecraft in order to provide contingency water at a substantial mass savings when compared to stored emergency water supplies. The system uses activated carbon treatment (for urine) followed by forward osmosis (FO). The LWC-WRS recovers water from a variety of contaminated sources by directly processing it into a fortified (electrolyte and caloric) drink. Primary target water sources are urine, seawater, and other on board vehicle waters (often referred to as technical waters). The product drink provides hydration, electrolytes, and caloric requirements for crew consumption. The system hardware consists of a urine collection device containing an activated carbon matrix (Stage 1) and an FO membrane treatment element (or bag) which contains an internally mounted cellulose triacetate membrane (Stage 2).

The Lightweight Contingency (LWC) Urine System is a contingency urine recovery system that produces a liquid food product. It does this on an individual (personal) basis thus removing the concerns associated with shared urine recycle. The system uses activated carbon treatment followed by forward osmosis (FO) to provide a hydration and electrolyte fluid (a sports drink) for crew consumption. The system hardware consists of an initial urine collection device containing an activated carbon matrix. This is followed by transfer of the treated urine into an FO membrane treatment cell. The FO treatment cell consists of a 2 L plastic bag. This FO bag is a robustly constructed intravenous (IV) surgical fluid drip bag equipped with input and output ports and an internally mounted cellulose triacetate membrane. All components are light weight disposable plastic, the system is potentially wearable, and it uses no electrical power.

The Vapor Phase Catalytic Ammonia Removal (VPCAR) system is being developed to recycle water for future NASA Exploration Missions [1,2,3,4,5]. Reduced gravity testing of the VPCAR System has been initiated to identify any potential problems with microgravity operation. Two microgravity testing campaigns have been conducted on NASA's C-9B Reduced Gravity Aircraft. These tests focused on the fluid dynamics of the unit's Wiped-Film Rotating Disk (WFRD) evaporator. The experiments used a simplified system to study the process of forming a thin film on a rotating disk. The configuration simulates the application of feed in the VPCAR's WFRD evaporator. The first round of aircraft testing, which was completed in early 2006, indicated that a problem with microgravity operation of the WFRD existed. It was shown that in reduced gravity the VPCAR wiper did not produce a uniform thin film [6]. The film was thicker near the axis of rotation where centrifugal forces are small.

The Vapor Phase Catalytic Ammonia Removal (VPCAR) technology has been previously discussed as a viable option for the Exploration Water Recovery System. This technology integrates a phase change process with catalytic oxidation in the vapor phase to produce potable water from exploration mission wastewaters. A developmental prototype VPCAR was designed, built and tested under funding provided by a National Research Announcement (NRA) project. The core technology, a Wiped Film Rotating Device (WFRD) was provided by Water Reuse Technologies under the NRA, whereas Hamilton Sundstrand Space Systems International performed the hardware integration and acceptance test of the system. Personnel at the Ames Research Center performed initial systems test of the VPCAR using ersatz solutions. To assess the viability of this hardware for Exploration Life Support (ELS) applications, the hardware has been modified and tested at the MSFC ECLS Test Facility.

Direct osmotic concentration (DOC) is a membrane treatment process for reclamation of space craft wastewater. It incorporates a novel system architecture that includes a forward osmosis (FO) and reverse osmosis (RO) subsystem for hygiene (gray) water, and a membrane distillation subsystem for the treatment of urine and humidity condensate. The products of these subsystems are combined and then post-treated by a catalytic oxidation subsystem. This paper documents progress made during the second year of a three year Rapid Technology Development Team (RTDT) effort.

NASA is currently developing two new human rated launch systems. They are the Crew Exploration Vehicle (CEV) and the Lunar Surface Access Module (LSAM). Both of these spacecraft will require new life support systems to support the crew. These life support systems can also be designed to reduce the mass required to keep humans alive in space. Water accounts for about 80% of the mass required to keep a person alive. As a result recycling water offers a high return on investment. Recycling water can also increase mission safety by providing an emergency supply of drinking water. This paper evaluates the potential benefits of two wastewater treatment technologies that have been designed to reduce the mass of the CEV and LSAM missions. For a 3 day CEV mission to the International Space Station (ISS) this approach could reduce the mass required to provide drinking water by 65% when compared to stored water. For an 18 day Lunar mission a mass savings of 70% is possible.

Direct osmotic concentration (DOC) has been identified as a potential wastewater treatment process for potable reuse in advanced life support systems (ALSS). As a result, further development of the DOC process is being supported by a NASA Rapid Technology Development Team (RTDT) program. DOC is an integrated membrane system combining three unique membrane separation processes including forward osmosis (FO), membrane distillation (MD), and reverse osmosis (RO) that is designed to treat separate wastewater streams comprising hygiene wastewater, humidity condensate, and urine. An aqueous phase catalytic oxidation (APCO) process is incorporated as post treatment for the product water. In an ongoing effort to improve the DOC process and make it fully autonomous, further development of the three membrane technologies is being pursued.

This study introduces new concepts in the function and placement of membrane based water treatment processes in Exploration Life Support (ELS) System design. These differences are in both form and function and have the potential to radically alter the current paradigms of thought within the ELS research community with regards to the limitations of conventional membrane water treatment. More importantly, they have the potential to change the placement of water processing by quite literally moving it “out of the box”, or in the case of ELS, the standard rack volume. Two possible systems, extremely small scale personal urine treatment and recycle (CEV Lightweight Contingency Water Treatment) and a similar but scaled up habitat wall embedded membrane water treatment pouch, are used to demonstrate the concepts involved.

This paper describes the results of ground testing of a scroll pump with a potential of being a substitute for the current vacuum pump of the Vapor Phase Catalytic Ammonia Reduction (VPCAR). Assessments of the pressure-time, pump-down time, pump power and the pump noise were made for three configurations of the pump the first of which was without the gas ballast, the second with the gas ballast installed but not operating and the third with the gas ballast operating. The tested scroll pump exhibited optimum characteristics given its mass and power requirements. The pump down time required to reach a pressure of 50 Torr ranged from 60 minutes without the ballast to about 120 minutes with the gas ballast operational. The noise emission and the pump power were assessed in this paper as well.

Presented is a synopsis of ongoing research into the development of techniques and hardware required to produce useable quantities of astrobiology relevant biomass under controlled and repeatable laboratory conditions. This study has developed microbial habitats (referred to as digesters, due to their biomass production function) capable of sustaining microbial communities under low temperature, high salt, high sulfate, anaerobic conditions. This set of basic conditions is necessary to develop biomass material that is analog to the biomass that would be present in subsurface brine habitats on Mars or Europa, from the perspective of several critical biochemical properties.

The Vapor Phase Catalytic Ammonia Removal (VPCAR) system is being developed to recycle water for future NASA Exploration Missions. Testing was recently conducted on NASA's C-9B Reduced Gravity Aircraft to determine the microgravity performance of a key component of the VPCAR water recovery system. Six flights were conducted to evaluate the fluid dynamics of the Wiped-Film Rotating Disk (WFRD) distillation component of the VPCAR system in microgravity, focusing on the water delivery method. The experiments utilized a simplified system to study the process of forming a thin film on a disk similar to that in the evaporator section of VPCAR. Fluid issues are present with the current configuration, and the initial alternative configurations were only partial successful in microgravity operation. The underlying causes of these issues are understood, and new alternatives are being designed to rectify the problems.

Dewatering of wet waste during space exploration missions is important for crew safety as it stabilizes the waste. It may also be used to recover water and serve as a preconditioning step for waste compaction. A thermoelectric cooler (TEC)- driven lyophilizer is under development at NASA Ames Research Center for this purpose. It has three major components: (i) an evaporator section where water vapor sublimes from the frozen waste, (ii) a condenser section where this water vapor deposits as ice, and (iii) a TEC section which serves as a heat pump to transfer heat from the condenser to the evaporator. This paper analyses the heat and mass transfer processes in the lyophilizer in an effort to understand the ice formation behavior in the condenser. The analysis is supported by experimental observations of ice formation patterns in two different condenser units.

One of the largest single mass penalties required to support the human exploration of Mars is the surface habitat structural mass. Reducing the amount of structural material that must be launched from Earth to provide a habitat will reduce the cost of future missions. This paper describes the use of physical chemical technologies to produce high-density polyethylene for use as structural/construction materials from Mars atmospheric carbon dioxide. The formation of polyethylene from Mars carbon dioxide is based on the use of the Sabatier and modified Fischer Tropsch reactions. The system describe can be fully integrate with planned Mars in situ propellant production concepts.

Mixed liquid/solid wastes, including feces, water processor effluents, and food waste, can be lyophilized (freeze-dried) to recover the water they contain and stabilize the solids that remain. Our previous research has demonstrated the potential benefits of using thermoelectric heat pumps to build a lyophilizer for processing waste in microgravity. These results were used to build a working prototype suitable for ground-based human testing. This paper describes the prototype design and presents results of functional and performance tests.

This paper describes the results of performance testing of the Vapor Phase Catalytic Ammonia Removal (VPCAR) technology. The VPCAR technology is currently being developed by NASA as a Mars transit vehicle water recycling system. NASA has recently completed a grant to develop a next generation VPCAR system. This grant concluded with the shipment of the final deliverable from Water Reuse Technology Inc. to NASA on August 31, 2003. This paper presents the results of initial performance testing of the VPCAR-EDU. Mass, power, volume, and acoustic measurements are reported. Product water purity analysis for a Mars transit mission and a planetary base simulated wastewater feeds are also reported.

This paper presents the results of a program to develop the next generation Vapor Phase Catalytic Ammonia Removal (VPCAR) system. VPCAR is a spacecraft water recycling system designed by NASA and constructed by Water Reuse Technology Inc. The technology has been identified by NASA to be the next generation water recycling system [1]. It is designed specifically for a Mars transit vehicle mission. This paper provides a description of the process and an evaluation of the performance of the new system. The equivalent system mass (ESM) is calculated and compared to the existing state-of-the art. A description of the contracting mechanism used to construct the new system is also provided.

This paper presents results of research on a solid waste dryer, based of the process of lyophilization, which recovers water and stabilizes solid waste. A lyophilizer has been developed and tested that uses thermoelectric heat pumps (TECs) to recycle heat during drying. The properties of TECs facilitate direct measurement of heat flow rates, and heat flow data are used to evaluate a heat and mass transfer model of the thermoelectric lyophilizer. Data are consistent with the theoretical model in most respects. Practical problems such as insulation and vacuum maintenance are minor in this system. However, the model’s assumption of a uniformly retreating ice layer during drying is valid only for the first 30% of water removed. Beyond this point, a shrinking core or lens model is more appropriate. Heat transfer to the shrinking core surrounded by dried material is slow.

For wastewater treatment applications, membrane processes are known to provide excellent treatment but are subject to failure due to membrane fouling. The Direct Osmotic Concentration (DOC) system evaluated in this study provides a membrane based primary treatment process capable of overcoming this problem. A full scale test apparatus containing full scale test module membrane cells has been developed and has undergone preliminary testing that provides a basis for comparison with other primary water recycle process concepts. This study confirms and extends the initial testing of this hardware and determines the required improvements to the existing test mo dules. These improvements, in addition to future testing, are intended to complete the validation of the concept and mature the hardware to the point that human rated test equipment design and development can be based directly on the test module derived data.