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Particulate matter in the air has become the focus of increased attention due to the concern of potential health effects. Among other sources, automotive vehicles are seen as a major contributor of fine particles. At present there is limited information available relating either to the number or size distribution of automotive particle emissions and detailed evidence has still to be established. To develop an understanding in the area of automotive particulate emissions a programme was carried out concentrating on tailpipe emissions as measured at the regulated particulate sampling point in a dilution tunnel. A previous literature study by CONCAWE had identified analytical techniques considered to be suitable for this application and which are capable of measuring both mass and number size distributions. Several variations of these techniques are available in the research field and the programme aimed to assess and compare their operation and performance.