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The objective of this work was to establish whether two detergent-type additives(A and B) influence the drop size and evaporation of two Diesel fuels (1 and 2) under Diesel engine conditions. Two experiments were performed: visualization of liquid and vapor fuel by the exciplex technique in a motored single-cylinder engine and measurement of the Sauter mean diameter, total drop cross sectional area and total drop volume by laser diffraction in a spray chamber. The same Diesel injector and pump system were used in the two experiments. The engine tests were carried out using a high aromatic content fuel (1) particularly suited for the exciplex studies. These studies showed that additive A yielded a lower vapor signal than additive B, which in turn gave a lower vapor signal than untreated fuel. Spray chamber results were obtained for both fuel 1 and 2. Additive A reduced the evaporation of fuel 1 whereas additive B gave a smaller and less consistent affect.