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Nowadays, SC is recognized as a key element of hybrid energy storage system in modern energy supply chain for electric vehicles (EVs). Co9S8 as a promising electrode material attracts much attention for supercapacitor owing to its superior electrochemical capacity. However, its poor stability and electronic conductivity, which result in inferior cycling performance and rate capability, have seriously limited the practical application of Co9O8 in supercapacitors. In this article, Co9S8 nanoparticles were embedded in reduced graphene oxide (rGO) via a simple anneal approach as high efficient and stable electrodes for SCs. The Co9S8/rGO composites were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray diffraction (XRD). The Co9S8 nanoparticles were inserted tightly between the rGO layers due to strong intermolecular forces, preventing the cluster in reduction process of rGO from graphene oxide (GO).