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Journal Article

Characterization of Damaging Biodiesel Deposits and Biodiesel Samples by Infrared Spectroscopy (ATR-FTIR) and Mass Spectrometry (TOF-SIMS)

2016-10-24
2016-01-9078
Biodiesel contains a variety of compounds, depending on the production and the provenance of the fuel. During the production process and usage, some of these compounds can form deposits (nozzle tip deposits or internal diesel injector deposits: “IDID”), which may lead to severe problems, such as corrosion, filter blockage and other technical issues. To deal with these difficulties, it is essential to exactly determine the components of these deposits. Most analytical methods used before, require complex preparations and result in limited information of the deposit material. Using infrared microscopy (ATR-FTIR: Attenuated-Total-Reflection Fourier-Transform-Infrared-Spectroscopy) or mass spectrometry (TOF-SIMS: Time-of-Flight Secondary-Ion-Mass-Spectrometry), a direct analysis of the original deposit material is possible.
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