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For better understanding, model development and its validation of in-cylinder soot formation processes of Gasoline Direct Injection (GDI) engines, visualization of piston surface fuel wetting, vaporization and soot formation processes of in-cylinder pool fire via high-speed UV (266nm) and visible (445nm) laser shadowgraphy was attempted in an optically accessible Rapid Compression and Expansion Machine (RCEM). A direct-injection, spark-ignition and single-shot combustion event was achieved in the RCEM under engine-equivalent, simplified and well-defined conditions operated with engine speed 600 rpm, compression ratio 9.0, equivalence ratio 0.9 and natural aspiration. The tested fuel was composed of 70% iso-octane and 30% toluene by volume and the UV absorption by toluene enabled visualization of the in-cylinder fuel distribution.