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The optimization of the mixture formation represents great potential to decrease fuel consumption and emissions of spark-ignition engines. The injector and the nozzle are of major importance in this concern. In order to adjust the nozzle geometry according to the requirements an understanding of the physical transactions in the fuel spray is essential. In particular, the primary spray break-up is still described inadequately due to the difficult accessibility with optical measuring instruments. This paper presents a methodology for the characterization of the nozzle-near spray development, which substantially influences the entire spray shape. Single hole injectors of the gasoline direct injection (GDI) with different nozzle hole geometries have been investigated in a high pressure chamber by using the MIE scattering technique. To examine the spray very close to the nozzle exit a long-distance microscope in combination with a Nd:YAG-laser was used.