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Comparing with port-fuel-injection (PFI) engine, the fuel sprays in spark-ignition direct-injection (SIDI) engines play more important roles since they significantly influence the combustion stability, engine efficiency as well as emission formations. In order to design higher efficiency and cleaner engines, further research is needed to understand and optimize the fuel spray atomization and vaporization. This paper investigates the atomization and evaporation of n-pentane, gasoline and surrogate fuels sprays under realistic SIDI engine conditions. An optical diagnostic technique combining high-speed Mie scattering and Schlieren imaging has been applied to study the characteristics of liquid and vapor phases inside a constant volume chamber under various operating conditions. The effects of ambient temperature, fuel temperature, and fuel type on spray atomization and vaporization are analyzed by quantitative comparisons of spray characteristics.