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The United States Environmental Protection Agency (U.S. EPA) National Enforcement Investigations Center (NEIC) has developed a test method for the analysis of washcoat material in small engine catalytic converters. Each small engine catalytic converter contains a metallic monolith. Each metallic monolith is removed from its outer casing, manually disassembled, and then separated into washcoat and substrate. The washcoat material is analyzed for platinum group metals (PGMs) using X-ray fluorescence (XRF) spectrometry. Results from the XRF analysis are used to calculate PGM ratios in the washcoat. During monolith disassembly, care is taken to minimize loss of washcoat or substrate, but some material is inevitably lost. The recovered washcoat mass does not necessarily equal the quantity of washcoat that was present in the intact catalytic converter.