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Recently, there has been increasing interest in catalysts with smaller volume for a Urea Selective Catalytic Reduction (SCR) system especially for use in heavy duty vehicles. In this study, several new concepts were developed in order to improve the deNOx performance of the SCR catalysts over a wide range of operating temperatures and this resulted in a compact SCR system. First, the urea decomposition process in diesel exhaust gas was elucidated. Several kinds of urea decomposition catalysts were investigated and the material which showed the best performance in NH3 (ammonia) formation was used to improve the low temperature performance of Cu-zeolite catalysts. Second, the method of reducing the amount of NH3 slip was investigated. It is well known that the amount of ammonia slip after the Urea-SCR system must be under 10 ppm and therefore materials with lower NH3 slip are preferred.