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The present paper deals with the development and evaluation of a new semi-empirical, pseudo-multi-zone model capable of estimating NOx emissions for various types of diesel engines and also different engine configurations. The specific model is physically based due to the use of the first thermodynamic law and the consideration of combustion chemistry and dissociation of the combustion products during the closed part of the engine cycle. The model estimates the fuel burning rate through Heat Release Rate Analysis of the measured cylinder pressure which is then coupled to a simplified multi-zone approach, assuming that each element of fuel burns individually at controlled conditions having from this point on its own history inside the combustion chamber. From this procedure, a simplified multi-zone semi-empirical model is developed, that accounts for the temperature distribution inside the combustion chamber and its evolution during an engine operating cycle.