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This paper reports the findings from an experimental investigation of the engine cooling jacket filling process for a medium duty off-highway diesel engine to characterise the physical processes that lead to the occurrence of trapped air. The motivation for the project was to provide knowledge and data to aid the development of a computational design tool capable of predicting the amount and location of trapped air in a cooling circuit following a fill event. To quantify the coolant filling process, a transparent replica of a section of the cylinder head cooling core was manufactured from acrylic to allow the application of optical diagnostic techniques. Experimentation has characterised the coolant filling process through the use of three optical techniques. These include the two established methods of High-Speed Imaging and Particle Image Velocimetry (PIV), as well as a novel approach developed for tracking the liquid-air interface during the fill event.