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Various polymer-based coatings are applied on piston skirt to reduce friction loss between the piston skirt and cylinder bore which is one of main factors of energy loss in an automotive engine system. These coatings generally consist of polymer binder (PAI) and solid lubricants (graphite or MoS₂) for low friction property. On the other hand, the present study found that PTFE as a solid lubricant and nano diamond as hard particles can be used to improve the low friction and wear resistance simultaneously. In the process of producing coating material, diamond particles pulverized to a nano size tend to agglomerate. To prevent this, silane (silicon coupling agent) treatment was applied. The inorganic functional groups of silane are attached to the nano diamond surface, which keep the diamond particles are apart.