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Gasoline homogeneous charge compression ignition (HCCI) can achieve high efficiency and extremely low NOX emissions. However, the working condition range of HCCI is limited by knock occurring during engine operation. To achieve an expanded HCCI working condition range, it is necessary to explore a method predicting knock cases accurately to avoid knock occurring. Based on a DI-HCCI engine with ethanol/gasoline mixed fuel, the knock cases under different conditions have been investigated. In-cylinder pressure signals are used to identify the knock cases and the knock oscillations are extracted with fast Fourier transform (FFT). The effects of the ethanol proportion in the fuel and air/fuel ratio on the characteristics of knock have been studied. The results have shown that the knock parameters, such as maximum frequency, start point angle and the duration, have close relationship with the knock intensity.