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Atmospheric pressure plasma sources are new devices for modifying the surface condition of engineering materials such as thermoplastic and thermoset-based composites. Because they operate at ambient conditions, these plasma systems can be used on a production line as a pre-treatment solution prior to painting or adhesive bonding to significantly improve adhesion strength. However, their efficient use requires sound understanding on how they modify the surface state of materials and, by the same token, how these modifications can be detected and quantified as regards their ability to provide high-strength adhesive joints. Polypropylene, since it is one of the most difficult-to-bond thermoplastic polymers and, at the same time, one of the most interesting polymers for the automotive industry (due to low cost, widespread use in the formulation of composites, lightweight and recyclability), was used in this paper as a model polymer.