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Simultaneous crank-angle-resolved measurements of gasoline concentration and gas temperature were made with two-color mid-infrared (mid-IR) laser absorption in a production spark-ignition engine (Nissan MR20DE, 2.0L, 4 cyl, MPI with premium gasoline). The mid-IR light was coupled into and out of the cylinder using fiber optics incorporated into a modified spark plug. The absorption line-of-sight was a 5.3 mm optical path located closely adjacent to the ignition spark providing spatially resolved absorption. Two sensor wavelengths were selected in the strong bands associated with the carbon-hydrogen (C-H) stretching vibration near 3.4 μm, which have an absorption ratio that is strongly temperature dependent. Fuel concentration and temperature were determined simultaneously from the absorption at these two wavelengths.