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Future synthetic diesel fuels will likely involve mixtures of straight and branched alkanes, possibly with aromatic additives to improve lubricity and durability. To simulate these future fuels, this study examined the combustion characteristics of binary mixtures of 50%, 70%, and 90% isododecane in hexadecane, and of 50%, 70%, and 80% toluene in hexadecane using a single-cylinder research diesel engine with variable injection timing. These binary blends were also compared to operation with commercial petroleum diesel fuel, military petroleum jet fuel, and five current synthetic Fischer-Tropsch diesel and jet fuels. The synthetic diesel and jet fuels showed reasonable similarity with many of the combustion metrics to mid-range blends of isododecane in hexadecane. Stable diesel combustion was possible even with the 80% toluene and 90% isododecane blends; in fact, operation with 100% isododecane was achieved, although with significantly advanced injection timing.