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To meet increasingly stringent diesel exhaust emissions requirements, original equipment manufacturers (OEMs) have introduced common rail fuel injection systems that develop pressures of up to 2000 bar (30,000 psi). In addition, fuel delivery schemes have become more complicated, often involving multiple injections per cycle. Containing higher pressures and allowing for precise metering of fuel requires very tight tolerances within the injector. These changes have made injectors more sensitive to fuel particulate contamination. Recently, problems caused by internal diesel injector deposits have been widely reported. In this paper, the results of an investigation into the chemical nature and probable sources of these deposits are discussed. Using an array of techniques, internal deposits were analyzed from on a number of sticking injectors from the field and from OEM test stands in North America.

Deposit formation is an issue of great significance in a broad range of applications where lubricants are exposed to high temperatures. Lube varnish causes valve-sticking, bearing failure and filter blockage which can lead to considerable equipment downtime and high maintenance costs. Recently this has become a pressing issue in the stationary power generation industry. In order to investigate the chemistry leading to varnish, three samples of varnish-coated components from the lube/hydraulic systems of gas turbines from the field were obtained, along with information on the commercially available formulated oils which were used. Samples of these three fresh oils were analysed by a variety of chromatographic and spectroscopic techniques, which confirmed chemical identity of aminic and/or phenolic antioxidants, corrosion inhibitors and antiwear components. The varnish-coated turbine components were also investigated by these methods.