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Copper is almost inevitable functional filler in the brake-material and efforts to replace it are continuing since it is now known as a hazard to the aquatic life. It is always desirable to search for ingredients for Cu-free brake-pads, which will be beneficial for friction-related properties and especially fade resistance. Attapulgite, is a mineral which was proven to be an excellent substitute for asbestos in brake-pads long back. However, hardly anything in details is reported on its exact role in controlling tribo-properties of friction materials (FMs). It was of interest, if it can be helpful in enhancing the performance of Cu-free FMs. Hence, in this work a series of brake-pads (five types) was formulated and developed with increasing amount of attapulgite (0, 5, 10 and 15 wt. %) by compensating with inert barite particles in Cu-free FMs. The parent composition was fixed and instead of Cu powder, 10 wt.% stainless steel powder was used.

Metallic particles in brake-friction materials (FMs) play a vital role in improving mainly strength, friction level, thermal conductivity and hence resistance to fade during braking operations. Although Copper was the most efficient and popular metallic ingredient in FMs, it is being phased out because of its proven threat to the aquatic life in the form of wear debris. Hardly any successful efforts are reported in open literature barring few on in the authors’ laboratory. It is well-known that the size and shape of particles affect the performance of composites apart from their type, concentration, etc. In this paper, Ferritic stainless steel (SS 434) particles were selected as a theme ingredient in two forms, first particulate (SSP) with two sizes, larger (30-45 micron) and smaller (10-20 micron) and also in the form of swarf. The aim was to investigate the size and shape effect of these ingredients when used to manufacture the brake-pads on the performance properties.

Graphite plays a crucial role in friction materials, since it has good thermal conductivity, lubricity and act as a friction modifier. The right type, amount, shape, and size of the particles control the performance of the brake-pads. The theme of the study was investigating the influence of size of graphite particles (having all other specifications identical) on performance properties of brake-pads containing graphite particles in the average size of 60 μm, 120 μm, 200 μm and 400 μm. Physical, mechanical and chemical characterization of the developed brake-pads was done. The tribological performance was studied using a full- scale inertia brake dynamometer following a Japanese automobile testing standard (JASO C406). Tribo-performance in terms of fade resistance, friction stability and wear resistance were observed best for smaller graphite particles. It was concluded that smaller size serves best for achieving best performance properties barring compressibility.

The binder in friction materials (FMs) plays a very crucial role which binds all the ingredients firmly so that they can function the way they were supposed to do. The type and amount of binder, both are very critical for manipulating the desired performance properties, which mainly include friction and its sensitivity towards operating parameters, wear resistance, counter-face friendliness, noise, vibration etc. Although a lot is reported on the influence of types of resins on tribo-performance of FMs, hardly any paper pertains to paint this on a bigger canvas with more detailed understanding of the amount of resin in FMs on the performance properties. The present study addresses these aspects by developing brake-pads with identical composition but varying in amount (wt. %) of straight phenolic resins (6, 8, 10 and 12) by compensating the difference with barite, a space filler. The ingredients did not contain asbestos, Copper, Zinc, etc. and hence were environment friendly.

Non-Asbestos Organic (NAO) brake- material research has been significant in the last decade in an attempt to replace the conventional semi-metallic and asbestos based materials. Influence of ingredients in this multi-ingredient (generally 10-25 in different proportions) system on performance properties, however, is still not thoroughly researched area because of complexity involved and needs intensive efforts to understand this aspect. Graphite is one of the most important and almost inevitable ingredients in friction materials. A wide variety of graphite varying in origin, particle size, crystallinity, thermal conductivity etc. is used by the industry. An in-depth and systematic study on the influence of size of graphite on tribo-performance, however, is not available.

Phenolics or their modified versions are invariably used as binder materials for friction composites which consist of multiple ingredients. However, phenolics are known for their inherent serious problems such as; poor shelf life, which poses constraints for storage and transportation; evolution of harmful volatiles leading to voids, cracks and environmental pollution etc. In order to overcome these, three new thermoset able resins having oxazine ring were synthesized in the laboratory. These resins proved to be free from the above mentioned drawbacks. These were tribo-evaluated to explore the possibility of replacing currently used phenolics in friction materials. In order to evaluate their tribo-potential as friction materials, friction formulations (non-asbestos organic NAO) based on these resins were developed in the laboratory in the form of brake-pads and tensile specimens.

Rising scarcity of conventional fuels has forced the development of bio-origin alternative fuels for the existing power generating machinery. These new alternative fuels need to be investigated for their long-term effect on the engine hardware. The biodiesel developed from vegetable oil has been used to partially replace the conventional mineral diesel fuel for diesel engine application. Experimental condition monitoring Study indicated lower wear of vital parts for the biodiesel blend fuelled engine pointing towards inherent lubricity properties of the biodiesel fuel. This phenomenon was experimentally verified in the present investigations. Series of experiments were conducted on SRV optimol wear tester by sliding a pin made of piston material against a disc made of cylinder liner and the lubrication was provided by the selected fuel blends.